Mechanics of Advanced Composite Structures

Mechanics of Advanced Composite Structures

Effect of Aspect Ratio on the Workability of AA6082/Metakaolin/Nano Silicon Nitride Composites: An Experimental Investigation and Predictive Modeling using RSM and ANN

Document Type : Research Article

Authors
1 Department of Production Engineering, PSG College of Technology, Coimbatore, 641004, Tamil Nadu, India
2 Department of Rural & Entrepreneurship Development, National Institute of Technical Teachers Training and Research, NITTTR, Chennai-600113, Tamil Nadu India
3 Department of Mechanical Engineering, Dr. Mahalingam College of Engineering and Technology, Pollachi 642003, Tamil Nadu, India
4 Department of Mechanical Engineering, Gharda Institute of Technology, Khed, Ratnagiri, 415708, Maharashtra, India
Abstract
Understanding the impact of aspect ratio on the deformation and load-bearing capacity of aluminium matrix composites is crucial in tailoring their forming performance. In this study, aluminium alloy (AA) 6082/Metakaolin (MK)/nano silicon nitride (Si₃N₄) composites containing 7.5 wt.% MK and 1.5 wt.% Si₃N₄ were fabricated using ultrasonic cavitation-assisted stir casting and tested under quasi-static compression with cylindrical specimens of aspect ratios 0.5, 1, and 1.5 in both as-cast and T6 heat-treated conditions. The results showed that lower aspect ratios significantly enhanced workability. The as-cast composite at aspect ratio 0.5 sustained compressive deformation up to a 50% reduction in height without visible cracks, achieving a maximum axial stress of 573.25 MPa. The T6 heat-treated samples exhibited a maximum compressive strength of 543.31 MPa and fractured at lower strain due to embrittlement caused by eutectic Si and Mg₂Si phases. Microstructural analysis indicated pore closure as the governing deformation mechanism in as-cast specimens, while brittle fracture dominated the T6 samples. Instantaneous strain hardening exponent (nᵢ) and strength coefficient (kᵢ) trends confirmed contributions from both matrix and geometric work hardening during deformation. In order to predict the workability parameters for different aspect ratios and loadings, response surface methodology (RSM) and artificial neural network (ANN) were employed. ANN yielded superior prediction accuracy for the workability parameters compared to RSM. These findings confirm that aspect ratio strongly controls the deformation mechanisms, with shorter cylindrical specimens offering optimum workability for practical forming operations.
Keywords
Subjects

[1]      Kumar, A., Singh, V.P., Singh, R.C., Chaudhary, R., Kumar, D. and Mourad, A.H.I., 2024. A review of aluminum metal matrix composites: fabrication route, reinforcements, microstructural, mechanical, and corrosion properties. Journal of Materials Science, 59(7), pp. 2644-2711. https://doi.org/10.1007/s10853-024-09398-7
[2]      Wu, X. and Zhang, W., 2024. A review on aluminum matrix composites' characteristics and applications for automotive sector. Heliyon, 10, e38576. https://doi.org/10.1016/j.heliyon.2024.e38576  
[3]      Sarmah, P. and Gupta, K., 2024. Recent advancements in fabrication of metal matrix composites: A systematic review. Materials, 17(18), p.4635. https://doi.org/10.3390/ma17184635
[4]      Khalid, M.Y., Umer, R. and Khan, K.A., 2023. Review of recent trends and developments in aluminium 7075 alloy and its metal matrix composites (MMCs) for aircraft applications. Results in Engineering, 20, p.101372. https://doi.org/10.1016/j.rineng.2023.101372
[5]      Bright, R.J., Selvakumar, G., Sumathi, M. and Lenin, N., 2019. Development, mechanical characterization and analysis of dry sliding wear behavior of AA6082–Metakaolin metal matrix composites. Materials Research Express, 6(12), p.126516. https://doi.org/10.1088/2053-1591/ab52aa
[6]      Hillary, J.J.M., Sundaramoorthy, R., Ramamoorthi, R. and Chelladurai, S.J.S., 2022. Investigation on microstructural characterization and mechanical behaviour of aluminium 6061–CSFA/sicp hybrid metal matrix composites. Silicon, 14(17), pp. 11561-11576. https://doi.org/10.1007/s12633-022-01881-7
[7]      Kumar, K.R., Pridhar, T. and Balaji, V.S., 2018. Mechanical properties and characterization of zirconium oxide (ZrO2) and coconut shell ash (CSA) reinforced aluminium (Al 6082) matrix hybrid composite. Journal of Alloys and Compounds, 765, pp. 171-179. https://doi.org/10.1016/j.jallcom.2018.06.177
[8]      Gupta, V., Singh, B. and Mishra, R.K., 2021. Tribological characteristics of AA7075 composites reinforced with rice husk ash and carbonized eggshells. Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications235(11), pp.2600-2613. https://doi.org/10.1177/14644207211025810
[9]      Kamatchi, R.M., Muraliraja, R., Vijay, J., Bharathi, C.S., Eswar, M.K. and Padmanabhan, S., 2023. Synthesis of Newly Formulated Aluminium Composite through Powder Metallurgy using Waste Bone Material. In E3S Web of Conferences (Vol. 399, p. 03016). EDP Sciences. https://doi.org/10.1051/e3sconf/202339903016
[10]  Bright, R.J. and Hariharasakthisudhan, P., 2022. Mechanical characterization and analysis of tensile fracture modes of ultrasonically stir cast Al6082 composites reinforced with Cu powder premixed Metakaolin particles. Frattura ed Integrita Strutturale16(62), pp.426-438. https://doi.org/10.3221/IGF-ESIS.62.29
[11]  Aydın, F., 2024. Recent Progress in Aluminium Matrix Composites: A Review on Tribological Performance. Transactions of the Indian Institute of Metals, 77(8), pp.1907-1922. https://doi.org/10.1007/s12666-024-03306-y  
[12]  Hariharasakthisudhan, P., Sudhan H.H., Karthik, S., Sathickbasha, K., Surya Rajan, B., 2022. Quasi-static compression behavior and microstructure changes in low-cost AA6061 composites. Proceedings of the Institution of Mechanical Engineers. Part C, journal of mechanical engineering science. 236(9), pp. 4876-4884. https://doi.org/10.1177/09544062211055339
[13]  Bright, R.J., Selvakumar, G., Hariharasakthisudhan, P. and Sumathi, M., 2022. Influence of nano-Si 3 N 4 (P) hybridization on the mechanical and quasi-static compression behaviour of AA6082-Metakaolin composites. Metallic Materials/Kovove Materialy, 60(3). https://doi.org/10.31577/km.2022.3.191
[14]  Dikshit, S., Gurjar, V., Dasgupta, R., Chaturvedi, S., Pathak, K.K. and Jha, A.K., 2010. Studies on cold upsetting behaviour of AA2014-based metal matrix composites, FEM simulation, and comparison with experimental results. Journal of materials science, 45, pp.4174-4179. https://doi.org/10.1007/s10853-010-4507-3
[15]  Narayanasamy, R. and Pandey, K.S., 1997. Phenomenon of barrelling in aluminium solid cylinders during cold upset-forming. Journal of Materials processing technology, 70(1-3), pp. 17-21. https://doi.org/10.1016/S0924-0136(97)00035-6
[16]  Narayanasamy, R., Ramesh, T. and Prabhakar, M., 2009. Effect of particle size of SiC in aluminium matrix on workability and strain hardening behaviour of P/M composite. Materials Science and Engineering: A, 504(1-2), pp. 13-23. https://doi.org/10.1016/j.msea.2008.11.037
[17]  Narayanasamy, R., Selvakumar, N. and Pandey, K.S., 2007. Phenomenon of instantaneous strain hardening behaviour of sintered Al–Fe composite preforms during cold axial forming. Materials & design, 28(4), pp. 1358-1363. https://doi.org/10.1016/j.matdes.2006.01.020
[18]  Narayanasamy, R., Anandakrishnan, V. and Pandey, K.S., 2008. Effect of geometric work-hardening and matrix work-hardening on workability and densification of aluminium–3.5% alumina composite during cold upsetting. Materials & Design, 29(8), pp. 1582-1599. https://doi.org/10.1016/j.matdes.2007.11.006
[19]  Narayanasamy, R., Ramesh, T. and Pandey, K.S., 2006. Workability studies on cold upsetting of Al–Al2O3 composite material. Materials & design, 27(7), pp.566-575. https://doi.org/10.1016/j.matdes.2004.12.005
[20]  Sumathi, M., Selvakumar, N. and Narayanasamy, R., 2012. Workability studies on sintered Cu–10SiC preforms during cold axial upsetting. Materials & Design, 39, pp. 1-8. https://doi.org/10.1016/j.matdes.2012.02.004
[21]  Sivasankaran, S., Sivaprasad, K., Narayanasamy, R. and Iyer, V.K., 2010. Effect of strengthening mechanisms on cold workability and instantaneous strain hardening behavior during grain refinement of AA 6061-10 wt.% TiO2 composite prepared by mechanical alloying. Journal of Alloys and Compounds, 507(1), pp.236-244. https://doi.org/10.1016/j.jallcom.2010.07.168
[22]  Jeyasimman, D. and Narayanasamy, R., 2016. Effect of coarse grain content on microstructure, cold workability and strain hardening behavior of trimodaled AA 6061 nanocomposites reinforced with multi-walled carbon nanotubes. Advanced Powder Technology, 27(4), pp. 1845-1851. http://dx.doi.org/10.1016/j.apt.2016.06.018
[23]  Taha, M.A., El-Mahallawy, N.A. and El-Sabbagh, A.M., 2008. Some experimental data on workability of aluminium-particulate-reinforced metal matrix composites. Journal of Materials Processing Technology, 202(1-3), pp. 380-385. https://doi.org/10.1016/j.jmatprotec.2007.07.047
[24]  Thangadurai, K.R. and Asha, A., 2014. Densification behavior in forming of stir casted aluminium boron carbide composite perform during cold upsetting. Applied Mechanics and Materials, 592, pp. 117-121. https://doi.org/10.4028/www.scientific.net/AMM.592-594.117
[25]  Sadhasivam, R.S., Ramanathan, K., Ravichandran, M. and Jayaseelan, C., 2022. Experimental investigations on microstructure, properties and workability behavior of zinc oxide reinforced Al–Si–Mg matrix composites. Silicon14(5), pp. 2175-2187. https://doi.org/10.1007/s12633-021-01012-8
[26]  Sivasankaran, S., Narayanasamy, R., Ramesh, T. and Prabhakar, M., 2009. Analysis of workability behavior of Al–SiC P/M composites using backpropagation neural network model and statistical technique. Computational Materials Science47(1), pp. 46-59. https://doi.org/10.1016/j.commatsci.2009.06.013
[27]  Hassani, A., Bagherpour, E. and Qods, F., 2014. Influence of pores on workability of porous Al/SiC composites fabricated through powder metallurgy+ mechanical alloying. Journal of Alloys and Compounds, 591, pp. 132-142. http://dx.doi.org/10.1016/j.jallcom.2013.12.205
[28]  Krishna, C.H., Dumpala, R., Davidson, M.J., Srinivasaraju, P. and Srinivasarao, G., 2020. Analysis of anisotropy in the upsetting process of AA2014 cast alloy embedded with fly ash. Proceedings of the Institution of Mechanical Engineers, Part C: Journal of Mechanical Engineering Science, 234(14), pp. 2833-2841. https://doi.org/10.1177/0954406220911389
[29]  Sivaraj, M. and Selvakumar, N., 2017. Effect of particle size on the deformation behaviour of sintered Al–TiC nano composites. Transactions of the Indian Institute of Metals, 70, pp. 2093-2102. https://doi.org/10.1007/s12666-016-1030-5
[30]  Raj, A.M., Selvakumar, N., Narayanasamy, R. and Kailasanathan, C., 2013. Experimental investigation on workability and strain hardening behaviour of Fe–C–Mn sintered composites with different percentage of carbon and manganese content. Materials & Design, 49, pp. 791-801.  http://dx.doi.org/10.1016/j.matdes.2013.02.002
[31]  Chen, Y., Wang, L., Feng, Z. and Zhang, W., 2021. Effects of heat treatment on microstructure and mechanical properties of SLMed Sc-modified AlSi10Mg alloy. Progress in Natural Science: Materials International, 31(5), pp. 714-721. https://doi.org/10.1016/j.pnsc.2021.08.003